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Oil Analysis - Physical Analysis

This involves a visual assessment of lube oils to identify gross contamination. Large metal and dirt particles and foreign bodies that are too big to be analysed by ICP-OES would go unnoticed without this simple check.

To simplify matters we have developed an arbitrary numerical scale that differentiates between types of visual contamination in oils. The scale appears on the back of every hard copy report we produce and can also be viewed below:

Appearance Rating Description of the Lubricant
10 Clear and Bright
20 Dark
30 Hazy
40 Cloudy
50 Emulsified (Milky)
60 Free Water
70 Solid Debris
80 Solid Debris and Free Water

Viscosity

The resistance to flow is measured by the time taken for a given volume of oil to flow under gravity between 2 points in a calibrated viscometer tube.

Viscosity measurements are essential to establish the correct grade of the oil in use, eg SAE 30 or 15w40. Slight changes in viscosity are to be expected during use, but abnormal changes must be detected and reported.

Abnormalities are indicative of one or more of the following problems:

Overheating

Fuel Dilution

High Insolubles

Excessive use

General contaminants

Wrong Oil Grade

All lubricating oils have a standard unused oil viscosity which is used to determine tolerances in the analysis of the in-service oil:

A 15% change from the unused is considered to be cautionary and a 20% change considered abnormal. For example an oil of ISO 100 grade will be subject to the following limits:

Normal - between 85Cst and 115Cst (Centistokes, the units of kinematic viscosity)

Caution - between 80Cst and 85Cst or between 115Cst and 120Cst

Serious - less than 80Cst or more than 120Cst

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